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EPA/OAR RIN: 2060-AW19 Publication ID: Spring 2024 
Title: ●Revisions to EPA Method 325A and Method 325B 
Abstract:

On December 1, 2015, the EPA finalized the residual risk and technology review of the Petroleum Refinery source categories regulated national emission standards for hazardous air pollutants (80 FR 75178). As part of that action, the EPA also finalized a fence line monitoring work practice standard to improve the management of fugitive emissions and finalized EPA Methods 325A/B (40 CFR part 63, Appendix A) to support the work practice. EPA’s Method 325A describes the collection of volatile organic compounds (VOCs) at or inside a facility property boundary or from fugitive and area emission sources using passive (diffusive) tube samplers (PS). The concentration of airborne VOCs at or near these potential fugitive- or area-emission sources may be determined using this method in combination with Method 325B. Companion Method 325B (Sampler Preparation and Analysis) describes preparation of sampling tubes, shipment and storage of exposed sampling tubes, and analysis of sampling tubes collected using either this passive sampling procedure or alternative active (pumped) sampling methods. More recently the use of Methods 325A/B were proposed to be used for a suite of compounds in the Hazardous Organic NESHAP or HON (88 FR 25080). Specifically, EPA proposed to require fence line monitoring of benzene, chloroprene, 1,3-butadiene, and ethylene dichloride measured in accordance with Methods 325A/B and indicated that EPA would be revising EPA Method 325B to incorporate new information on uptake rates and to incorporate the sorbents (88 FR 25143). The EPA is proposing to revise Methods 325 A and B to incorporate new information on uptake rates, to incorporate the sorbents, and to reflect current laboratory best practices.

 
Agency: Environmental Protection Agency(EPA)  Priority: Substantive, Nonsignificant 
RIN Status: First time published in the Unified Agenda Agenda Stage of Rulemaking: Proposed Rule Stage 
Major: No  Unfunded Mandates: No 
CFR Citation: 40 CFR 63 app. A   
Legal Authority: Clean Air Act    42 U.S.C. 7401 et seq.   
Legal Deadline:  None
Timetable:
Action Date FR Cite
NPRM  08/00/2024 
Final Rule  06/00/2025 
Additional Information: EPA-HQ-OAR-2023-0634.
Regulatory Flexibility Analysis Required: No  Government Levels Affected: None 
Federalism: No 
Included in the Regulatory Plan: No 
RIN Data Printed in the FR: No 
Agency Contact:
Ned Shappley
Environmental Protection Agency
Office of Air and Radiation
109 T.W. Alexander Drive, Mail Code E143-02,
Research Triangle Park, NC 27709
Phone:919 541-7903
Email: shappley.ned@epa.gov